(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Base Information

Chemical Name:(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone
CAS No.:156161-83-0
Molecular Formula:C₁₈H₂₄O₆
Molecular Weight:336.385
Hs Code.:

(2S-trans)-2-ortho-methoxybenzyl-5-<<<pivaloyl>oxy>methyl>dihydro-3-(2H)furanone

Synonyms:(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Suppliers and Price of (2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Chemical Property:

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Technology Process of (2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

There total 8 articles about (2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 156161-72-7
ortho-methoxybenzyl-3-deoxy-5-O-pivaloyl-α-D-threo-pentofuranoside

: 156161-83-0
(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 1h;
DOI:10.1016/S0040-4020(01)80628-1

Reference yield:

: 53081-35-9
methyl 3-deoxy-α-D-threo-pentofuranoside

: 156161-83-0
(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / conc. H₂SO₄ / Ambient temperature

2: 1.) 4 Angstroem MS, 2.) trimethylsilyl triflate / 1.) CH₂Cl₂, r.t., 1.5 h, 2.) CH₂Cl₂, -5 deg C, 2 h

3: 96 percent / 1M NaOMe / methanol / 14 h

4: 84 percent / pyridine / 96 h / 4 °C

5: 91 percent / Dess-Martin-periodinane / CH₂Cl₂ / 1 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; 4 Angstroem MS; sulfuric acid; sodium methylate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)80628-1

Reference yield:

: 612-16-8
(2-methoxyphenyl)methanol

: 156161-83-0
(2S-trans)-2-ortho-methoxybenzyl-5-<<oxy>methyl>dihydro-3-(2H)furanone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 4 Angstroem MS, 2.) trimethylsilyl triflate / 1.) CH₂Cl₂, r.t., 1.5 h, 2.) CH₂Cl₂, -5 deg C, 2 h

2: 96 percent / 1M NaOMe / methanol / 14 h

3: 84 percent / pyridine / 96 h / 4 °C

4: 91 percent / Dess-Martin-periodinane / CH₂Cl₂ / 1 h

With pyridine; trimethylsilyl trifluoromethanesulfonate; 4 Angstroem MS; sodium methylate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)80628-1