benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside

Base Information

• Chemical Name: benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside
• CAS No.: 32849-00-6
• Molecular Formula: C₆₈H₅₄O₁₉
• Molecular Weight: 1175.17

Synonyms:benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside

Chemical Property of benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside

Chemical Property:

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Technology Process of benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside

There total 2 articles about benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzoyl chloride (98-88-4) + LACTOSE (5965-66-2) → 1,2,3,6-tetra-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranose (4710-82-1,4780-99-8,14200-60-3,15098-62-1,18311-29-0,32849-00-6,41545-58-8,66101-71-1,91280-47-6,114718-48-8,151123-95-4,151123-96-5,41093-36-1)

Guidance literature:

With pyridine; at 0 - 20 ℃; for 12h;

Reference yield:

benzoyl chloride (98-88-4) + LACTOSE (5965-66-2) → 1,2,3,6-tetra-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranose (4710-82-1,4780-99-8,14200-60-3,15098-62-1,18311-29-0,32849-00-6,41545-58-8,66101-71-1,91280-47-6,114718-48-8,151123-95-4,151123-96-5,41093-36-1) + benzoyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-α-D-glucopyranoside (41545-58-8)

Guidance literature:

With pyridine; dmap; at 65 ℃; Inert atmosphere;

Reference yield: 91.0%

benzoyl (2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-(1->4)-(2,3,6-tri-O-benzoyl)-D-glucopyranoside (32849-00-6) → 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl)-β-D-glucopyranosyl azide (1385026-74-3)

Guidance literature:

With gold(III) tribromide; trimethylsilylazide; In dichloromethane; at 55 ℃; for 2h;

DOI:10.3762/bjoc.14.56

upstream raw materials:

benzoyl chloride

LACTOSE

Downstream raw materials:

ethyl 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1-thio-α-D-glucopyranoside

ethyl 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-1-thio-β-D-glucopyranoside

2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1-4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

(O-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl)-trichloroacetimidate

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