(E)-3-(p-tolyl)allyl benzoyloxycarbamate

Base Information

Chemical Name:(E)-3-(p-tolyl)allyl benzoyloxycarbamate
CAS No.:1424055-82-2
Molecular Formula:C₁₈H₁₇NO₄
Molecular Weight:311.337
Hs Code.:

Synonyms:(E)-3-(p-tolyl)allyl benzoyloxycarbamate

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Chemical Property of (E)-3-(p-tolyl)allyl benzoyloxycarbamate

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Technology Process of (E)-3-(p-tolyl)allyl benzoyloxycarbamate

There total 4 articles about (E)-3-(p-tolyl)allyl benzoyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97585-04-1,20511-20-0,24393-49-5
ethyl (E)-3-(4-methylphenyl)acrylate

: 1424055-82-2
(E)-3-(p-tolyl)allyl benzoyloxycarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere

2: acetonitrile / 20 °C

3: triethylamine / tetrahydrofuran / 0 °C

With diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1002/chem.201603977

Reference yield:

: 1424055-69-5
C₁₁H₁₃NO₃

: 98-88-4
benzoyl chloride

: 1424055-82-2
(E)-3-(p-tolyl)allyl benzoyloxycarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃;
DOI:10.1002/chem.201603977

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1424055-82-2
(E)-3-(p-tolyl)allyl benzoyloxycarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere; Schlenk technique

1.2: 2.5 h / 0 °C / Inert atmosphere; Schlenk technique

2.1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere

3.1: acetonitrile / 20 °C

4.1: triethylamine / tetrahydrofuran / 0 °C

With sodium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; toluene; acetonitrile; 1.1: |Horner-Wadsworth-Emmons Olefination / 1.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1002/chem.201603977