1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI)

Base Information

Chemical Name:1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI)
CAS No.:113305-00-3
Molecular Formula:C₈H₁₁NO₂
Molecular Weight:153.181
Hs Code.:
Mol file:113305-00-3.mol

Synonyms:1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI)

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Technology Process of 1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI)

There total 2 articles about 1-Pyrrolidinecarboxylicacid,3-ethenylidene-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 113304-87-3
(5-Trimethylsilanyl-pent-3-ynyl)-carbamic acid methyl ester

: 113305-00-3
3-Vinylidene-pyrrolidine-1-carboxylic acid methyl ester

Guidance literature:: In formic acid; for 17h; Ambient temperature;
DOI:10.1016/S0040-4039(00)95494-7

Reference yield:

: 101195-67-9
5-Trimethylsilanyl-pent-3-ynylamine

: 113305-00-3
3-Vinylidene-pyrrolidine-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂

2: 54 percent / formic acid / 17 h / Ambient temperature

With triethylamine; In formic acid; dichloromethane;
DOI:10.1016/S0040-4039(00)95494-7