C₃₄H₃₉Cl₂N₃O₁₂

Base Information

Chemical Name:C₃₄H₃₉Cl₂N₃O₁₂
CAS No.:1276614-72-2
Molecular Formula:C₃₄H₃₉Cl₂N₃O₁₂
Molecular Weight:752.603
Hs Code.:

C<sub>34</sub>H<sub>39</sub>Cl<sub>2</sub>N<sub>3</sub>O<sub>12</sub>

Synonyms:C₃₄H₃₉Cl₂N₃O₁₂

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Chemical Property of C₃₄H₃₉Cl₂N₃O₁₂

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Technology Process of C₃₄H₃₉Cl₂N₃O₁₂

There total 10 articles about C₃₄H₃₉Cl₂N₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₃₁N₃O₁₀

: 41490-13-5
4-(benzyloxy)-3,5-dichlorobenzoicacid

: 1276614-72-2
C₃₄H₃₉Cl₂N₃O₁₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2010.12.068

Reference yield:

: 1276614-42-6
C₂₁H₃₂N₂O₇

: 1276614-72-2
C₃₄H₃₉Cl₂N₃O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1: AD-mix-β; water / tert-butyl alcohol / 0 - 20 °C

2: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / -78 - 20 °C

3: dmap; triethylamine / dichloromethane / 2.5 h / -78 - -10 °C

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 20 °C

5: Jones reagent / acetone / 1.5 h / 0 - 20 °C

6: tetrahydrofuran; diethyl ether

7: sodium azide / N,N-dimethyl-formamide / 36 h / 20 °C

8: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 760.05 Torr

9: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; Jones reagent; sodium azide; AD-mix-β; palladium 10% on activated carbon; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; water; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2010.12.068

Reference yield:

: 1276614-66-4
C₂₇H₄₈N₂O₉Si

: 1276614-72-2
C₃₄H₃₉Cl₂N₃O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; triethylamine / dichloromethane / 2.5 h / -78 - -10 °C

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 5 h / 20 °C

3: Jones reagent / acetone / 1.5 h / 0 - 20 °C

4: tetrahydrofuran; diethyl ether

5: sodium azide / N,N-dimethyl-formamide / 36 h / 20 °C

6: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 760.05 Torr

7: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0 - 20 °C

With dmap; Jones reagent; sodium azide; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2010.12.068