3,5-Dichloro-4-phenylmethoxybenzoic acid

Base Information

• Chemical Name: 3,5-Dichloro-4-phenylmethoxybenzoic acid
• CAS No.: 41490-13-5
• Molecular Formula: C14H10 Cl2 O3
• Molecular Weight: 297.138
• Mol file: 41490-13-5.mol

Synonyms:4-Benzyloxy-3,5-dichlorobenzoicacid; NSC 212202

Chemical Property of 3,5-Dichloro-4-phenylmethoxybenzoic acid

Chemical Property:

• Vapor Pressure: 1.91E-08mmHg at 25°C
• Boiling Point: 438°Cat760mmHg
• Flash Point: 218.7°C
• Density: 1.411g/cm³

Purity/Quality:

99% ^*data from raw suppliers

3,5-Dichloro-4-phenylmethoxybenzoicacid 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3,5-Dichloro-4-phenylmethoxybenzoic acid

There total 7 articles about 3,5-Dichloro-4-phenylmethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-benzyloxy-3,5-dichlorobenzoic acid methyl ester (536974-83-1) → 4-(benzyloxy)-3,5-dichlorobenzoicacid (41490-13-5)

Guidance literature:

With potassium hydroxide; In ethanol; for 48h; Inert atmosphere; Reflux;

DOI:10.1016/j.ejmech.2020.112866

Reference yield: 96.0%

→ 4-(benzyloxy)-3,5-dichlorobenzoicacid (41490-13-5)

Guidance literature:

Reference yield: 74.0%

3,5-dichloro-4-hydroxybenzoic acid (3336-41-2) + benzyl bromide (100-39-0) → 4-(benzyloxy)-3,5-dichlorobenzoicacid (41490-13-5)

Guidance literature:

3,5-dichloro-4-hydroxybenzoic acid; benzyl bromide; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

With potassium hydroxide; In methanol; for 1h; Reflux;

With hydrogenchloride; In methanol; water; pH=2 - 3;

upstream raw materials:

ethyl 3,5-dichloro-4-(benzyloxy)benzoate

3,5-dichloro-4-hydroxybenzoic acid

benzyl bromide

4-benzyloxy-3,5-dichlorobenzoic acid methyl ester

Downstream raw materials:

(4R,5S)-3-benzyl 4-methyl 5-((2R,5S)-1-(tert-butoxycarbonyl)-2-(methoxycarbonyl)-5-((S)-2-(tert-butyldimethylsilyloxymethyl)-2-(4-benzyloxy-3,5-dichlorobenzamido)ethyl)pyrrolidin-2-yl)-2,2-dimethyloxazolidine-3,4-dicarboxylate

3,5-dichloro-4-benzoxybenzoic chloride

methyl (1S,5R,7aR)-5-((S)-2-(4-(benzyloxy)-3,5-dichlorobenzamido)-3-methoxy-3-oxopropyl)-1-((R)-1-((tert-butoxycarbonyl)amino)-2-methoxy-2-oxoethyl)-3-oxodihydro-1H,3H-pyrrolo[1,2-c]oxazole-7a(5H)-carboxylate

C₃₄H₃₉Cl₂N₃O₁₂

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