3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

Base Information

Chemical Name:3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]
CAS No.:865482-58-2
Molecular Formula:C₂₅H₃₀N₄O₁₁
Molecular Weight:562.533
Hs Code.:

Synonyms:3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

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Chemical Property of 3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

Chemical Property:

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Technology Process of 3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

There total 4 articles about 3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52450-18-7
3'-amino-3'-deoxythymidine

: 865482-58-2
3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

Guidance literature:: Multi-step reaction with 3 steps

1: 83.8 percent / ethanol / 1 h / 20 °C

2: 73 percent / pyridine; DMAP / 30 h / 20 - 30 °C

3: DCC / dioxane; pyridine / 2 h / 20 °C

With pyridine; dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; ethanol;
DOI:10.1002/hlca.200390295

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 654678-74-7
3'-{[(tert-butoxy)carbonyl]amino}-3'-deoxythymidine 5'-(hydrogen butanedioate)

: 865482-58-2
3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; at 20 ℃; for 2h;
DOI:10.1002/hlca.200390295

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 865482-58-2
3'-{[(tert-butyl)carbonyl]amino}-3'-deoxythymidine 5'-O-[(4-nitrophenyl) butanedioate]

Guidance literature:: Multi-step reaction with 3 steps

1: 83.8 percent / ethanol / 1 h / 20 °C

2: 73 percent / pyridine; DMAP / 30 h / 20 - 30 °C

3: DCC / dioxane; pyridine / 2 h / 20 °C

With pyridine; dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; pyridine; ethanol;
DOI:10.1002/hlca.200390295