Technology Process of C28H23NO2
There total 6 articles about C28H23NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium carbonate;
In
tetrahydrofuran;
at 50 ℃;
for 36h;
Inert atmosphere;
DOI:10.1080/00397911003706982
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / tetrahydrofuran; hexane; water / -10 - 20 °C / Inert atmosphere
2: palladium diacetate; potassium carbonate / tetrahydrofuran / 36 h / 50 °C / Inert atmosphere
With
hydrogenchloride; palladium diacetate; potassium carbonate;
In
tetrahydrofuran; hexane; water;
2: Suzuki coupling;
DOI:10.1080/00397911003706982
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) chloride; potassium hydroxide / o-xylene; toluene / 48 h / 120 °C / Inert atmosphere
2: n-butyllithium / tetrahydrofuran; hexane / -78 - -10 °C / Inert atmosphere
3: hydrogenchloride / tetrahydrofuran; hexane; water / -10 - 20 °C / Inert atmosphere
4: palladium diacetate; potassium carbonate / tetrahydrofuran / 36 h / 50 °C / Inert atmosphere
With
hydrogenchloride; n-butyllithium; palladium diacetate; potassium carbonate; copper(l) chloride; potassium hydroxide;
In
tetrahydrofuran; hexane; o-xylene; water; toluene;
1: Ullmann reaction / 4: Suzuki coupling;
DOI:10.1080/00397911003706982