3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

Base Information

Chemical Name:3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine
CAS No.:102104-68-7
Molecular Formula:C₂₀H₃₄N₂O₄S
Molecular Weight:398.567
Hs Code.:

Synonyms:3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

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Chemical Property of 3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

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Technology Process of 3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

There total 3 articles about 3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 54767-81-6
5-(epoxyethyl)-1,2,3-tris(methoxy)benzene

: 88346-63-8
3-(6-aminohexyl)-1,3-thiazolidine

: 102104-68-7
3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

Guidance literature:: In isopropyl alcohol; for 22h; Heating;
DOI:10.1021/jm00390a011

Reference yield: 77.0%

: 54767-81-6
5-(epoxyethyl)-1,2,3-tris(methoxy)benzene

: 88346-63-8
3-(6-aminohexyl)-1,3-thiazolidine

: 2-(6-Thiazolidin-3-yl-hexylamino)-2-(3,4,5-trimethoxy-phenyl)-ethanol

: 102104-68-7
3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

Guidance literature:: In isopropyl alcohol; for 22h; Heating;
DOI:10.1002/jhet.5570220326

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 102104-68-7
3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / aq. sodium hydroxide (50 percent), tetrabuthylammonium bromide / CH₂Cl₂ / 96 h / 50 °C

2: 77 percent / propan-2-ol / 22 h / Heating

With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; isopropyl alcohol;
DOI:10.1002/jhet.5570220326