6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

Base Information

Chemical Name:6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione
CAS No.:849949-81-1
Molecular Formula:C₆₀H₅₃N₅O₇
Molecular Weight:956.11
Hs Code.:

Synonyms:6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

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Chemical Property of 6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

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Technology Process of 6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

There total 4 articles about 6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 849949-92-4
C₅₄H₄₄N₂O₈

: 5036-48-6
3-(1H-imidazol-1-yl)propan-1-amine

: 849949-81-1
6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: In tetrahydrofuran; at 60 ℃; for 24h;
DOI:10.1021/jm0493764

Reference yield:

: 849949-91-3
C₅₅H₄₇N₃O₇

: 849949-81-1
6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. KOH / ethanol; toluene / 20 °C

1.2: 80 percent / aq. citric acid / ethanol; toluene / 20 °C / pH 6

2.1: 80 percent / tetrahydrofuran / 24 h / 60 °C

With potassium hydroxide; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/jm0493764

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 849949-81-1
6-(3-imidazol-1-yl-propyl)-12-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6,7,12,13-tetrahydroindolo-[2,3-a]pyrrolo[3,4-c]carbazole-5,7-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / NaOH; Na₂SO₄ / acetonitrile / 24 h / 20 °C

2.1: aq. KOH / ethanol; toluene / 20 °C

2.2: 80 percent / aq. citric acid / ethanol; toluene / 20 °C / pH 6

3.1: 80 percent / tetrahydrofuran / 24 h / 60 °C

With potassium hydroxide; sodium hydroxide; sodium sulfate; In tetrahydrofuran; ethanol; toluene; acetonitrile;
DOI:10.1021/jm0493764