Technology Process of C19H17BrO5
There total 4 articles about C19H17BrO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen;
In
1,2-dichloro-ethane;
at 90 ℃;
for 24h;
Sealed tube;
DOI:10.1021/ja307497h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tris(diethylamino)sulfonium difluorotrimethylsiliconate / dichloromethane / -78 °C / Inert atmosphere
2: oxygen / 1,2-dichloro-ethane / 24 h / 90 °C / Sealed tube
With
tris(diethylamino)sulfonium difluorotrimethylsiliconate; oxygen;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja307497h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; triethylamine / tetrahydrofuran / -60 - 24 °C / Inert atmosphere
2: tris(diethylamino)sulfonium difluorotrimethylsiliconate / tetrahydrofuran / 1 h / -78 - 24 °C / Inert atmosphere
3: oxygen / 1,2-dichloro-ethane / 24 h / 90 °C / Sealed tube
With
copper(l) iodide; tris(diethylamino)sulfonium difluorotrimethylsiliconate; oxygen; triethylamine;
In
tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ja307497h