(1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

Base Information

• Chemical Name: (1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione
• CAS No.: 1192030-83-3
• Molecular Formula: C₄₄H₅₀O₇Si
• Molecular Weight: 718.962

Synonyms:(1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

Chemical Property of (1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

Chemical Property:

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Safty Information:

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Technology Process of (1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

There total 1 articles about (1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(1R,2R,4S)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-5-hydroxy-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione (1192030-70-8) + benzyl bromide (100-39-0) → (1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione (1192030-83-3)

Guidance literature:

With silver(l) oxide; In N,N-dimethyl-formamide; at 25 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ja9073694

Reference yield:

(1R,2R,4S)-5-(benzyloxy)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione (1192030-83-3) → C40H42O5Si

Guidance literature:

With hydrogenchloride; In methanol; water; at 50 ℃; for 4h; Inert atmosphere;

DOI:10.1021/ja9073694

upstream raw materials:

(1R,2R,4S)-1-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-5-hydroxy-4-((2-methoxyethoxy)methoxy)-2-methyl-1,2,3,4-tetrahydroanthracene-9,10-dione

benzyl bromide

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