9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Base Information

Chemical Name:9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine
CAS No.:1356682-47-7
Molecular Formula:C₂₂H₂₉BrN₄O₅Si
Molecular Weight:537.486
Hs Code.:

Synonyms:9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

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Chemical Property of 9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Chemical Property:

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Technology Process of 9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

There total 1 articles about 9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: hydrogen fluoride-pyridine

: 1356682-49-9
9-[2-O-(4-bromobenzyl)-3,5-o-(di-tert-butylsilanylidene)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

: 1356682-47-7
9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Guidance literature:: In tetrahydrofuran; ethyl acetate;

Reference yield:

: 1356682-47-7
9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1356682-55-7
9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Guidance literature:: In pyridine; hexane; ethyl acetate;

Reference yield:

: 1356682-47-7
9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

: 1356681-77-0
9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-[4-(pyridin-4-yl)benzyl]-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate; hexane; pyridine

2: potassium carbonate / ethyl acetate; hexane; 2-methyl-THF

With potassium carbonate; In pyridine; 2-methyl-THF; hexane; ethyl acetate;