9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Base Information

• Chemical Name: 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine
• CAS No.: 1356682-55-7
• Molecular Formula: C₄₃H₄₇BrN₄O₇Si
• Molecular Weight: 839.858

Synonyms:9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Chemical Property of 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

Chemical Property:

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Technology Process of 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

There total 1 articles about 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356682-47-7) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356682-55-7)

Guidance literature:

In pyridine; hexane; ethyl acetate;

Reference yield:

tris-(dibenzylideneacetone)dipalladium(0) (52409-22-0,51364-51-3) + (4-(N,N-dimethylamino)phenyl)-di-tert-butylphosphine (932710-63-9) + 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356682-55-7) + 2-(tributyltin)oxazole (145214-05-7) → 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-[4-(1,3-oxazol-2-yl)benzyl]-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356681-60-1)

Guidance literature:

In tetrahydrofuran; hexane; ethyl acetate;

Reference yield:

9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-(4-bromobenzyl)-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356682-55-7) + palladium diacetate (3375-31-3) + 4-pyridylboronic acid (1692-15-5) + 1,2-dichloro-ethane (107-06-2,52399-93-6) + catacxium A (321921-71-5) → 9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-[4-(pyridin-4-yl)benzyl]-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine (1356681-77-0)

Guidance literature:

With potassium carbonate; In 2-methyl-THF; hexane; ethyl acetate;

upstream raw materials:

9-[2-O-(4-bromobenzyl)-β-D-ribofuranosyl]-6-[2-(trimethylsilyl)ethoxy]-9H-purine

4,4'-dimethoxytrityl chloride

Downstream raw materials:

9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-[4-(1,3-oxazol-2-yl)benzyl]-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

9-{5-O-[bis(4-methoxyphenyl)(phenyl)methyl]-2-o-[4-(pyridin-4-yl)benzyl]-β-D-ribofuranosyl}-6-[2-(trimethylsilyl)ethoxy]-9H-purine

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