N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide
CAS No.:1620882-48-5
Molecular Formula:C₃₂H₃₀ClN₃O₄S₂
Molecular Weight:620.193
Hs Code.:

Synonyms:N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

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Technology Process of N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

There total 4 articles about N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: 1620727-53-8
3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)aniline

: 98-59-9
p-toluenesulfonyl chloride

: 1620882-48-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

Guidance literature:: 3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)aniline; With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;

p-toluenesulfonyl chloride; In dichloromethane; for 3h;
DOI:10.3390/molecules19022694

Reference yield:

: 121-51-7
3-nitrobenzenesulphonyl chloride

: 1620882-48-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C

1.2: 2 h

2.1: hydrogenchloride; tin(ll) chloride / ethanol / Reflux

3.1: triethylamine / dichloromethane / 0.17 h / 0 °C

3.2: 3 h

With hydrogenchloride; triethylamine; tin(ll) chloride; In ethanol; dichloromethane;
DOI:10.3390/molecules19022694

Reference yield:

: 1423771-99-6
8-Chloro-11-(1-((3-nitrophenyl)sulfonyl)piperidin-4-ylidene)-6,11-dihydro-5H-benzo[5,6]cyclohepta-[1,2-b]pyridine

: 1620882-48-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; tin(ll) chloride / ethanol / Reflux

2.1: triethylamine / dichloromethane / 0.17 h / 0 °C

2.2: 3 h

With hydrogenchloride; triethylamine; tin(ll) chloride; In ethanol; dichloromethane;
DOI:10.3390/molecules19022694