RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄

Base Information

• Chemical Name: RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄
• CAS No.: 143958-12-7
• Molecular Formula: BF₄*C₄₂H₄₈NO₃P₄Ru
• Molecular Weight: 926.618

Synonyms:RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄

Chemical Property of RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄

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Technology Process of RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄

There total 1 articles about RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾*BF₄^(1-)={RuH(CH₃CN)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + RuH2(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2) (143958-06-9) → RuH(CH3CN)(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2)(1+)*BF4(1-)={RuH(CH3CN)(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2)}BF4 (143958-12-7)

Guidance literature:

With acetonitrile; In dichloromethane; N2; HBF4*Et2O added to soln. of complex at -78°C; after 5 min CH3CN was added; warmed to room temp.;; concd.; pptd. from Et2O; filtered; washed with Et2O; dried in vacuo; elem. anal.;;

Reference yield:

RuH(CH3CN)(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2)(1+)*BF4(1-)={RuH(CH3CN)(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2)}BF4 (143958-12-7) → RuH(H2)(P(OCH2)3CC2H5)(P(C6H5)(CH2CH2P(C6H5)2)2)(1+) (143958-09-2)

Guidance literature:

With hydrogen;

upstream raw materials:

tetrafluoroboric acid diethyl ether

RuH₂(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)

Downstream raw materials:

RuH(H₂)(P(OCH₂)3CC₂H₅)(P(C₆H₅)(CH₂CH₂P(C₆H₅)2)2)⁽¹⁺⁾

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