methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

Base Information

Chemical Name:methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside
CAS No.:207602-68-4
Molecular Formula:C₂₂H₂₃F₃O₈S
Molecular Weight:504.481
Hs Code.:

Synonyms:methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

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Technology Process of methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

There total 3 articles about methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 207602-70-8
methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-β-D-galactopyranoside

: 207602-68-4
methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

Guidance literature:: With pyridine; In dichloromethane; at -20 - 0 ℃;
DOI:10.1071/C97153

Reference yield:

: 39946-32-2
methyl 2-O-benzyl-6-deoxy-β-D-galactopyranoside

: 207602-68-4
methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / triethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 5 h / -50 °C

2: 83 percent / pyridine / CH₂Cl₂ / -20 - 0 °C

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1071/C97153

Reference yield:

: 98-88-4
benzoyl chloride

: 207602-68-4
methyl 3-O-benzoyl-2-O-benzyl-6-deoxy-4-O-trifluoromethylsulfonyl-β-D-galactoside

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / triethylamine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 5 h / -50 °C

2: 83 percent / pyridine / CH₂Cl₂ / -20 - 0 °C

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1071/C97153