1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

Base Information

Chemical Name:1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole
CAS No.:124604-56-4
Molecular Formula:C₃₀H₂₇NO₂
Molecular Weight:433.55
Hs Code.:

Synonyms:1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

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Technology Process of 1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

There total 5 articles about 1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 24626-27-5
3,3-diphenylallyl chloride

: 124604-54-2
6-((trimethylsilyl)oxy)-1-oxo-2,3,3a,4,5,7a-hexahydropyrido<3,2,1-jk>carbazole

: 124604-56-4
1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

Guidance literature:: With tin(IV) chloride;
DOI:10.1021/jo00292a042

Reference yield: 80.0%

: 3923-51-1
1,1-diphenylprop-2-en-1-ol

: 124604-54-2
6-((trimethylsilyl)oxy)-1-oxo-2,3,3a,4,5,7a-hexahydropyrido<3,2,1-jk>carbazole

: 124604-56-4
1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -78 ℃; for 6h;
DOI:10.1021/jo00292a042

Reference yield:

: 703-80-0
3-acetylindole

: 124604-56-4
1,6-dioxo-6a-(3,3-diphenyl-2-propenyl)-2,3,3a,4,5,6,6a,7a-octahydropyrido<3,2,1-jk>carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / triethylamine / CH₂Cl₂ / 8 h / 0 °C

2: 1.) diisopropylethylamine, 2.) hexamethyldisilazane / 1.) CH₂Cl₂, 0 deg C, 4 h, 2.) toluene, 48 h, 270 deg C

3: 80 percent / TiCl₄ / CH₂Cl₂ / 6 h / -78 °C

With titanium tetrachloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1,1,3,3,3-hexamethyl-disilazane; In dichloromethane;
DOI:10.1021/jo00292a042