C₆H₁₀O₃C₆H₆SC₇H₆

Base Information

Chemical Name:C₆H₁₀O₃C₆H₆SC₇H₆
CAS No.:939050-49-4
Molecular Formula:C₁₉H₂₂O₃S
Molecular Weight:330.448
Hs Code.:

C<sub>6</sub>H<sub>10</sub>O<sub>3</sub>C<sub>6</sub>H<sub>6</sub>SC<sub>7</sub>H<sub>6</sub>

Synonyms:C₆H₁₀O₃C₆H₆SC₇H₆

Suppliers and Price of C₆H₁₀O₃C₆H₆SC₇H₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₁₀O₃C₆H₆SC₇H₆

Chemical Property:

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Technology Process of C₆H₁₀O₃C₆H₆SC₇H₆

There total 5 articles about C₆H₁₀O₃C₆H₆SC₇H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₁₀O₃(C₂H₂O)2C₆H₆S

: 939050-49-4
C₆H₁₀O₃C₆H₆SC₇H₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe; MeOH / 2 h / 20 °C

2.1: Bu₂SnO / toluene / 5 h / Heating

2.2: 83 percent / Bu₄NI / toluene / 12 h / 100 °C

With methanol; sodium methylate; di(n-butyl)tin oxide; In toluene;
DOI:10.1002/anie.200604031

Reference yield:

: 18546-25-3
6-O-p-tolylsulfonyl-3,4-di-O-acetyl-D-glucal

: 939050-49-4
C₆H₁₀O₃C₆H₆SC₇H₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaBr; NaHCO₃ / dimethylformamide / 12 h / 65 °C

2.1: 13.0 g / Bu₃SnH; AIBN / toluene / 1.5 h / 110 °C

3.1: HCl / toluene; ethyl acetate / 2.5 h / 0 °C

3.2: 45 percent / DIEA / CH₂Cl₂ / 1 h / 0 °C

4.1: NaOMe; MeOH / 2 h / 20 °C

5.1: Bu₂SnO / toluene / 5 h / Heating

5.2: 83 percent / Bu₄NI / toluene / 12 h / 100 °C

With hydrogenchloride; methanol; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; sodium hydrogencarbonate; sodium bromide; In ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.200604031

Reference yield:

: 363134-99-0
diacetyl-d-glucal-6-bromohydrin

: 939050-49-4
C₆H₁₀O₃C₆H₆SC₇H₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: 13.0 g / Bu₃SnH; AIBN / toluene / 1.5 h / 110 °C

2.1: HCl / toluene; ethyl acetate / 2.5 h / 0 °C

2.2: 45 percent / DIEA / CH₂Cl₂ / 1 h / 0 °C

3.1: NaOMe; MeOH / 2 h / 20 °C

4.1: Bu₂SnO / toluene / 5 h / Heating

4.2: 83 percent / Bu₄NI / toluene / 12 h / 100 °C

With hydrogenchloride; methanol; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; In ethyl acetate; toluene;
DOI:10.1002/anie.200604031