trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

Base Information

Chemical Name:trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}
CAS No.:132231-82-4
Molecular Formula:C₄₀H₃₈Cl₂O₄P₂Pt
Molecular Weight:910.673
Hs Code.:

Synonyms:trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

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Chemical Property of trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

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Technology Process of trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

There total 1 articles about trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 14873-63-3,15617-19-3,51921-56-3
trans-bis(benzonitrile)dichloroplatinum(II)

: (2,5-dimethoxybenzyl)diphenylphosphine

: 132231-82-4
PtCl₂(P(C₆H₅)2(C₆H₃(OCH₃)2))2

Guidance literature:: In dichloromethane; (N2); stirring (15 min); solvent redn., pptn. by dropwise addn. of Et2O; elem. anal.;
DOI:10.1039/a900610i

Reference yield: 96.0%

: 132231-82-4
PtCl₂(P(C₆H₅)2(C₆H₃(OCH₃)2))2

: Pt(OC₆H₃(OH)CH₂P(C₆H₅)2)2*1.5H₂O

Guidance literature:: With BBr₃; Na₂CO₃; In dichloromethane; (N2); addn. of BBr3 to Pt complex in CH2Cl2, stirring (16 h), solvent removal, addn. of MeOH and Na2CO3, stirring (3 h); filtration, washing (water), rinsing (Et2O), drying in air; elem. anal.;
DOI:10.1039/a900610i

Reference yield: 87.0%

: 132231-82-4
trans-{platinum(chloro)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

: 132231-84-6,132563-99-6
{platinum(iodo)2(2,5-dimethoxy-1-diphenylphosphino-benzene)2}

Guidance literature:: With KI; In acetone; stirring of the chloroplatinum-complex and KI in dry acetone for 20 h under dry dinitrogen; mixture of cis/trans-isomers (1:3) is obtained, elem. anal.;
DOI:10.1016/S0020-1693(00)84848-3