(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

Base Information

Chemical Name:(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide
CAS No.:852045-23-9
Molecular Formula:C₅₇H₆₅NO₆
Molecular Weight:860.146
Hs Code.:

Synonyms:(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

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Technology Process of (1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

There total 5 articles about (1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 852045-22-8
(1S,2R,3S,4R,5R,6S)-2,3,4,5,6-pentakis-benzyloxy-N-phenylethylcyclohexylamine

: 111-64-8
n-octanoic acid chloride

: 852045-23-9
(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/b411473f

Reference yield:

: 852045-20-6
(1s,2R,3S,4r,5R,6S)-2,3,4,5,6-pentakis(benzyloxy)cyclohexanamine

: 852045-23-9
(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium cyanoborohydride; acetic acid / methanol / 18 h / 20 °C

2: 82 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With sodium cyanoborohydride; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1039/b411473f

Reference yield:

: 868550-22-5,852045-19-3
(1S,2S,3R,4R,5S,6R)-1-azido-2,3,4,5,6-pentakis-benzyloxycyclohexane

: 852045-23-9
(1S,2R,3S,4R,5R,6S)-N-phenethyl-N-(2,3,4,5,6-pentakis-benzyloxycyclohexyl)octanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / 20 °C

2: 85 percent / sodium cyanoborohydride; acetic acid / methanol / 18 h / 20 °C

3: 82 percent / Et₃N / CH₂Cl₂ / 18 h / 20 °C

With lithium aluminium tetrahydride; sodium cyanoborohydride; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1039/b411473f