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C34H37F5N4O6S

Base Information
  • Chemical Name:C34H37F5N4O6S
  • CAS No.:1419386-60-9
  • Molecular Formula:C34H37F5N4O6S
  • Molecular Weight:724.749
  • Hs Code.:
C<sub>34</sub>H<sub>37</sub>F<sub>5</sub>N<sub>4</sub>O<sub>6</sub>S

Synonyms:C34H37F5N4O6S

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Chemical Property of C34H37F5N4O6S
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Technology Process of C34H37F5N4O6S

There total 16 articles about C34H37F5N4O6S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; Inert atmosphere;
Guidance literature:
Multi-step reaction with 4 steps
1: hydrogenchloride / ethyl acetate / 20 °C
2: N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice
3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 90 °C / Inert atmosphere
4: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere
With hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
Guidance literature:
Multi-step reaction with 7 steps
1: potassium tert-butylate / toluene / 3.5 h / 80 °C / Inert atmosphere; Cooling with ice
2: Lawessons reagent / toluene / 18 h / Inert atmosphere; Reflux
3: antimony(III) chloride; (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 18 h / 20 °C / Inert atmosphere; Cooling with ice
4: N-iodo-succinimide; trifluoroacetic acid / acetonitrile / 20 °C / Cooling with ice
5: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere
6: pyridine / dichloromethane / 3.33 h / 20 °C / Inert atmosphere; Cooling with ice
7: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,2-dimethoxyethane; water / 90 °C / Inert atmosphere
With Lawessons reagent; pyridine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate; antimony(III) chloride; boron tribromide; potassium carbonate; trifluoroacetic acid; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In 1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile;
upstream raw materials:

4-methoxylindanone

C14H16O2

C14H16OS

C14H16F2O

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