4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

Base Information

Chemical Name:4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde
CAS No.:348639-12-3
Molecular Formula:C₂₉H₁₈F₆O₂S₂
Molecular Weight:576.583
Hs Code.:

Synonyms:4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

There total 13 articles about 4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 636600-99-2
1,2-bis(2-methyl-5-(4-(2,5-dioxolanyl)phenyl)thiophen-3-yl)hexafluorocyclopentene

: 348639-12-3
4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

Guidance literature:: With water; pyridinium p-toluenesulfonate; In acetone; for 16h; Heating;
DOI:10.1002/chem.200304947

Reference yield: 65.0%

: 559-40-0
octaperfluorocyclopentene

: 550348-57-7
3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene

: 348639-12-3
4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

Guidance literature:: octaperfluorocyclopentene; 3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 7h;

With pyridinium p-toluenesulfonate; In water; acetone; for 48h; Reflux;
DOI:10.1021/jacs.8b13675

Reference yield: 63.0%

: 87199-17-5
4-formylphenylboronic acid,

: 159590-16-6
3,3'-(perfluorocyclopent-1-ene-1,2-diyl)bis(5-bromo-2-methylthiophene)

: 348639-12-3
4,4'-(4,4'-perfluorocyclopent-1-ene-1,2-diyl)bis(5-methylthiophene-4,2-diyl)dibenzaldehyde

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; at 75 ℃; for 36h;
DOI:10.1021/ma0504163