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3-methoxy-9-(4-methoxyphenyl)thioxanthenol

Base Information
  • Chemical Name:3-methoxy-9-(4-methoxyphenyl)thioxanthenol
  • CAS No.:476331-79-0
  • Molecular Formula:C21H18O3S
  • Molecular Weight:350.438
  • Hs Code.:
3-methoxy-9-(4-methoxyphenyl)thioxanthenol

Synonyms:3-methoxy-9-(4-methoxyphenyl)thioxanthenol

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Chemical Property of 3-methoxy-9-(4-methoxyphenyl)thioxanthenol
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Technology Process of 3-methoxy-9-(4-methoxyphenyl)thioxanthenol

There total 3 articles about 3-methoxy-9-(4-methoxyphenyl)thioxanthenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
1-bromo-4-methoxy-benzene; With magnesium; ethylene dibromide; In tetrahydrofuran; Heating;
3-methoxy-9H-thioxanthen-9-one; In tetrahydrofuran; for 3h; Further stages.; Heating;
DOI:10.1021/jo026009w
Guidance literature:
Multi-step reaction with 2 steps
1.1: 44 percent / H2SO4; SO2Cl2 / 3 h / 60 °C
2.1: Mg; ethylene dibromide / tetrahydrofuran / Heating
2.2: 59 percent / tetrahydrofuran / 3 h / Heating
With sulfuryl dichloride; sulfuric acid; magnesium; ethylene dibromide; In tetrahydrofuran; 1.1: Friedel-Crafts / 2.2: Grignard reaction;
DOI:10.1021/jo026009w
Guidance literature:
Multi-step reaction with 2 steps
1.1: 44 percent / H2SO4; SO2Cl2 / 3 h / 60 °C
2.1: Mg; ethylene dibromide / tetrahydrofuran / Heating
2.2: 59 percent / tetrahydrofuran / 3 h / Heating
With sulfuryl dichloride; sulfuric acid; magnesium; ethylene dibromide; In tetrahydrofuran; 1.1: Friedel-Crafts / 2.2: Grignard reaction;
DOI:10.1021/jo026009w
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