N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

Base Information

Chemical Name:N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride
CAS No.:474940-67-5
Molecular Formula:C₁₀H₉ClF₃NO
Molecular Weight:251.636
Hs Code.:

Synonyms:N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

Chemical Property:

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Technology Process of N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

There total 2 articles about N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 26819-14-7
N-(2,2,2-trifluoroethyl)-p-methoxybenzamide

: 474940-67-5
N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

Guidance literature:: With phosphorus pentachloride; In benzene; for 12h; Heating;
DOI:10.1039/b202005j

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 474940-67-5
N-(2,2,2-trifluoroethyl)-p-methoxybenzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / triethylamine / diethyl ether / 3 h / Heating

2: 65 percent / phosphorus pentachloride / benzene / 12 h / Heating

With phosphorus pentachloride; triethylamine; In diethyl ether; benzene;
DOI:10.1039/b202005j