(R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane
CAS No.:827608-90-2
Molecular Formula:C₂₂H₃₄B₂O₄
Molecular Weight:384.132
Hs Code.:

Synonyms:(R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

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Chemical Property of (R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

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Technology Process of (R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

There total 1 articles about (R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40339-20-6
buta-2,3-dienyl-benzene

: 73183-34-3
bis(pinacol)diborane

: 827608-90-2
(R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

: (S)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (3aR,8aR)-(-)-(2,2-dimethyl-4,4,8,8-tetraphenyl-tetrahydro-[1,3]dioxolo[4,5-e][1,3,2]dioxaphosphepin-6-yl)dimethylamine; In toluene; at 20 ℃; for 14h; Title compound not separated from byproducts;
DOI:10.1021/ja044167u

Reference yield:

: 827608-90-2
(R)-4,4,5,5-tetramethyl-2-(4-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)but-1-en-2-yl)-1,3,2-dioxaborolane

: C₂₈H₄₀B₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 9 h / 20 °C

2: Cs₂CO₃; H₂O / toluene / 12 h / 80 °C

With water; caesium carbonate; In toluene; 2: Suzuki-Miyaura cross-coupling;
DOI:10.1021/ol0616891