5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

Base Information

Chemical Name:5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline
CAS No.:426255-94-9
Molecular Formula:C₂₅H₁₉NO₄
Molecular Weight:397.43
Hs Code.:

Synonyms:5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

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Chemical Property of 5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

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Technology Process of 5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

There total 4 articles about 5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1-(4,6-dimethoxy-3-phenylindol-7-yl)-3-phenyl-2,3-epoxypropan-1-one

: 426255-94-9
5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 4h;
DOI:10.1021/jo010915b

Reference yield:

: 105776-29-2
4,6-dimethoxy-3-phenyl-1H-indole

: 426255-94-9
5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / phosphoryl chloride / 0 - 55 °C

2: 92 percent / sodium amide / tetrahydrofuran / 0.5 h

3: 82 percent / H₂O₂; NaOH / tetrahydrofuran; H₂O

4: 82 percent / KOH / H₂O; tetrahydrofuran / 4 h / 20 °C

With potassium hydroxide; sodium hydroxide; dihydrogen peroxide; sodium amide; trichlorophosphate; In tetrahydrofuran; water;
DOI:10.1021/jo010915b

Reference yield:

: 426255-82-5
1-(4,6-dimethoxy-3-phenylindol-7-yl)ethanone

: 426255-94-9
5-hydroxy-7,9-dimethoxy-1,4-diphenyl-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / sodium amide / tetrahydrofuran / 0.5 h

2: 82 percent / H₂O₂; NaOH / tetrahydrofuran; H₂O

3: 82 percent / KOH / H₂O; tetrahydrofuran / 4 h / 20 °C

With potassium hydroxide; sodium hydroxide; dihydrogen peroxide; sodium amide; In tetrahydrofuran; water;
DOI:10.1021/jo010915b