diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

Base Information

Chemical Name:diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate
CAS No.:1258428-89-5
Molecular Formula:C₅₁H₇₄FN₈O₁₃PS
Molecular Weight:1089.23
Hs Code.:

diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

Synonyms:diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

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Chemical Property of diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

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Technology Process of diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

There total 1 articles about diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1258428-88-4
4-(((S)-1-(((S)-1-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)amino)-3-(4-((bis(allyloxy)phosphoryl)oxy)-3-(fluoromethyl)phenyl)-1-oxopropan-2-yl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-4-oxobutanoic acid

: 194920-57-5
2-(2-(2-(5-(2-oxo-1,3,3a,4,6,6a-hexahydrothieno[3,4-d]imidazol-6-yl)pentanoylamino)ethoxy)ethoxy)ethylammonium 2,2,2-trifluoroacetate

: 1258428-89-5
diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;
DOI:10.1016/j.tet.2010.04.065

Reference yield: 90.0%

: 1258428-89-5
diallyl (4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohex-ahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetra-azapentacosyl)-2-(fluoromethyl)phenyl)phosphate

: 1258428-84-0
4-((2S,5S)-2-(((S)-1-amino-4-methyl-1-oxopentan-2-yl)carbamoyl)-5-benzyl-4,7,10,21-tetraoxo-25-((3aS,4S,6aR)-2-oxohexahydro-1H-thieno[3,4-d]imidazol-4-yl)-14,17-dioxa-3,6,11,20-tetraazapentacosyl)-2-(fluoromethyl)phenyl dihydrogen phosphate

Guidance literature:: With trimethylsilyl bromide; N,O-Bis(trimethylsilyl)trifluoroacetamide; In acetonitrile; at 20 ℃; Cooling with ice;
DOI:10.1016/j.tet.2010.04.065