N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine

Base Information

• Chemical Name: N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine
• CAS No.: 1263364-06-2
• Molecular Formula: C₂₅H₃₅N₉O₁₀
• Molecular Weight: 621.607

Synonyms:N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine

Chemical Property of N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine

Chemical Property:

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Technology Process of N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine

There total 1 articles about N₂-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H39N9O12 → N2-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine (1263364-06-2)

Guidance literature:

With ammonia; In methanol; dichloromethane; at 40 ℃; for 24h;

DOI:10.1002/hlca.201000253

Reference yield: 84.0%

N2-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine (1263364-06-2) + 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate (169049-82-5) → 2-(4-nitrophenyl)ethyl 5-{{{{2-{2-{2-{{9-(2'-deoxy-β-D-ribofuranosyl)-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}-6,9-dihydro-6-oxo-1H-purin-2-yl}amino}ethoxy}ethoxy}ethyl}amino}carbonyl}amino}-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate (1263364-07-3)

Guidance literature:

With pyridine; dmap; In N,N-dimethyl-formamide; at 70 ℃; for 0.75h;

DOI:10.1002/hlca.201000253

Downstream raw materials:

2-(4-nitrophenyl)ethyl 5-{{{{2-{2-{2-{{9-(2'-deoxy-β-D-ribofuranosyl)-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}-6,9-dihydro-6-oxo-1H-purin-2-yl}amino}ethoxy}ethoxy}ethyl}amino}carbonyl}amino}-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate

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