C₁₂H₁₄BrNO₄

Base Information

Chemical Name:C₁₂H₁₄BrNO₄
CAS No.:1357259-26-7
Molecular Formula:C₁₂H₁₄BrNO₄
Molecular Weight:316.151
Hs Code.:

C<sub>12</sub>H<sub>14</sub>BrNO<sub>4</sub>

Synonyms:C₁₂H₁₄BrNO₄

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Chemical Property of C₁₂H₁₄BrNO₄

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Technology Process of C₁₂H₁₄BrNO₄

There total 1 articles about C₁₂H₁₄BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 199328-35-3
ethyl 2-(4-bromo-2-nitrophenyl)acetate

: 74-88-4
methyl iodide

: 1357259-26-7
C₁₂H₁₄BrNO₄

Guidance literature:: ethyl 2-(4-bromo-2-nitrophenyl)acetate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;

Reference yield: 79.0%

: 1357259-26-7
C₁₂H₁₄BrNO₄

: 1314655-86-1
C₁₀H₁₀BrNO₄

Guidance literature:: C₁₂H₁₄BrNO₄; With water; potassium hydroxide; In tetrahydrofuran; methanol; at 80 ℃; for 5h;

With hydrogenchloride; In water; pH=2;

Reference yield:

: 1357259-26-7
C₁₂H₁₄BrNO₄

: 1357259-28-9
C₁₉H₂₈BrN₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; water / tetrahydrofuran; methanol / 5 h / 80 °C

1.2: pH 2

2.1: triethylamine / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

2.2: 3 h / 20 °C

3.1: triethylamine; HATU / dichloromethane / 0.25 h / 20 °C

3.2: 1 h / 20 °C

4.1: hydrogen / platinum on activated charcoal / methanol / 1034.32 Torr

With water; hydrogen; triethylamine; HATU; potassium hydroxide; platinum on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;