C₁₅H₂₄O₂C₁₀H₁₄O₄

Base Information

Chemical Name:C₁₅H₂₄O₂C₁₀H₁₄O₄
CAS No.:363139-98-4
Molecular Formula:C₂₅H₃₈O₆
Molecular Weight:434.573
Hs Code.:

C<sub>15</sub>H<sub>24</sub>O<sub>2</sub>C<sub>10</sub>H<sub>14</sub>O<sub>4</sub>

Synonyms:C₁₅H₂₄O₂C₁₀H₁₄O₄

Suppliers and Price of C₁₅H₂₄O₂C₁₀H₁₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₄O₂C₁₀H₁₄O₄

Chemical Property:

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Technology Process of C₁₅H₂₄O₂C₁₀H₁₄O₄

There total 14 articles about C₁₅H₂₄O₂C₁₀H₁₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 146746-58-9
1-bromo-2-methoxy-6-(methoxymethoxy)benzene

: 199180-19-3
cis-decaline

: 363139-98-4
C₁₅H₂₄O₂C₁₀H₁₄O₄

Guidance literature:: 1-bromo-2-methoxy-6-(methoxymethoxy)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -40 ℃; for 0.5h;

cis-decaline; In tetrahydrofuran; hexane; at -40 - -20 ℃; for 0.5h; Further stages.;
DOI:10.1021/ol016285h

Reference yield:

: 57234-28-3
1-methoxy-3-(methoxymethoxy)benzene

: 363139-98-4
C₁₅H₂₄O₂C₁₀H₁₄O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: t-BuLi; TMEDA / diethyl ether; pentane / 1 h / -78 °C

1.2: 73 percent / Br₂ / diethyl ether / 3 h / -78 - 0 °C

2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -40 °C

2.2: 97 percent / tetrahydrofuran; hexane / 0.5 h / -40 - -20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; In tetrahydrofuran; diethyl ether; hexane; pentane;
DOI:10.1021/ol016285h

Reference yield:

: 150-19-6
O-methylresorcine

: 363139-98-4
C₁₅H₂₄O₂C₁₀H₁₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: 91 percent / DIPEA / CH₂Cl₂ / 3 h / 20 °C

2.1: t-BuLi; TMEDA / diethyl ether; pentane / 1 h / -78 °C

2.2: 73 percent / Br₂ / diethyl ether / 3 h / -78 - 0 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -40 °C

3.2: 97 percent / tetrahydrofuran; hexane / 0.5 h / -40 - -20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; pentane;
DOI:10.1021/ol016285h