(1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol

Base Information

• Chemical Name: (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol
• CAS No.: 322640-31-3
• Molecular Formula: C₁₈H₂₈O₃
• Molecular Weight: 292.419

Synonyms:(1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol

Chemical Property of (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol

Chemical Property:

Purity/Quality:

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Technology Process of (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol

There total 3 articles about (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanone (322640-10-8) → (1R,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol + (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol (322640-31-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/ol0068243

Reference yield:

pulegone (89-82-7,90449-51-7) → (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol (322640-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: CuI / tetrahydrofuran

2: LiAlH₄ / tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; lithium aluminium tetrahydride; In tetrahydrofuran; 1: Grignard reaction;

DOI:10.1021/ol0068243

Reference yield:

2,4-dimethoxyphenylmagnesium bromide (138109-49-6) → (1S,2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanol (322640-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: CuI / tetrahydrofuran

2: LiAlH₄ / tetrahydrofuran / 12 h / 20 °C

With copper(l) iodide; lithium aluminium tetrahydride; In tetrahydrofuran; 1: Grignard reaction;

DOI:10.1021/ol0068243

upstream raw materials:

(2S,5R)-2-[1-(2,4-Dimethoxy-phenyl)-1-methyl-ethyl]-5-methyl-cyclohexanone

pulegone

2,4-dimethoxyphenylmagnesium bromide

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