Technology Process of C34H43N5O4Si
There total 6 articles about C34H43N5O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
N-(2-((tert-butyldimethylsilyl)oxy)ethyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline; C20H19BrN4O3;
With
potassium carbonate;
In
tetrahydrofuran; water;
at 20 ℃;
for 1h;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water;
at 20 - 70 ℃;
for 2.25h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; diphenyl phosphoryl azide / 18 h / Reflux
2.1: trifluoroacetic acid / dichloromethane / 12 h / 20 °C
3.1: triethylamine / toluene / 4 h / 0 - 100 °C
3.2: 14 h / 0 - 20 °C
4.1: potassium carbonate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere
4.2: 2.25 h / 20 - 70 °C / Inert atmosphere
With
diphenyl phosphoryl azide; potassium carbonate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 14 h / 100 °C / Inert atmosphere
2.1: 1H-imidazole / dichloromethane / 2 h / 0 °C
3.1: potassium carbonate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere
3.2: 2.25 h / 20 - 70 °C / Inert atmosphere
With
1H-imidazole; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium carbonate;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
