C₂₀H₂₇N₃O₄

Base Information

Chemical Name:C₂₀H₂₇N₃O₄
CAS No.:1338251-62-9
Molecular Formula:C₂₀H₂₇N₃O₄
Molecular Weight:373.452
Hs Code.:

C<sub>20</sub>H<sub>27</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₀H₂₇N₃O₄

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Chemical Property of C₂₀H₂₇N₃O₄

Chemical Property:

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Technology Process of C₂₀H₂₇N₃O₄

There total 8 articles about C₂₀H₂₇N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1338251-61-8
C₂₀H₂₉N₃O₅

: 1338251-62-9
C₂₀H₂₇N₃O₄

Guidance literature:: With pyridine; trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2011.07.087

Reference yield:

: 4395-98-6
4-cyanopiperidine

: 1338251-62-9
C₂₀H₂₇N₃O₄

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C

3: platinum(IV) oxide; hydrogen / acetic acid / 20 °C

4: sodium hydrogencarbonate / dichloromethane / 0 - 20 °C

5: water; sodium hydroxide / ethanol / Reflux

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

7: pyridine; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C

With pyridine; platinum(IV) oxide; water; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic anhydride; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.087

Reference yield:

: 1016258-69-7
1-tert-butyl 4-ethyl 4-(aminomethyl)piperidine-1,4-dicarboxylate

: 1338251-62-9
C₂₀H₂₇N₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / dichloromethane / 0 - 20 °C

2: water; sodium hydroxide / ethanol / Reflux

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C

4: pyridine; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C

With pyridine; water; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic anhydride; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.087