C₂₈H₁₈O₆

Base Information

Chemical Name:C₂₈H₁₈O₆
CAS No.:1332848-92-6
Molecular Formula:C₂₈H₁₈O₆
Molecular Weight:450.447
Hs Code.:

C<sub>28</sub>H<sub>18</sub>O<sub>6</sub>

Synonyms:C₂₈H₁₈O₆

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Chemical Property of C₂₈H₁₈O₆

Chemical Property:

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Technology Process of C₂₈H₁₈O₆

There total 9 articles about C₂₈H₁₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1332849-06-5
C₃₂H₂₆O₆

: 1332848-92-6
C₂₈H₁₈O₆

Guidance literature:: C₃₂H₂₆O₆; With potassium hydroxide; In tetrahydrofuran; ethanol; at 20 ℃; for 15.5h;

With trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1002/chem.201101015

Reference yield:

: 842120-12-1
1-hydroxy-2,5-diiodo-4-methoxybenzene

: 1332848-92-6
C₂₈H₁₈O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16.5 h / 60 °C

2.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4.1: potassium hydroxide / tetrahydrofuran; ethanol / 15.5 h / 20 °C

4.2: 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101015

Reference yield:

: 1332849-17-8
1,4-diiodo-2-methoxy-5-(3-triisopropylsilylprop-2-ynyloxy)benzene

: 1332848-92-6
C₂₈H₁₈O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3.1: potassium hydroxide / tetrahydrofuran; ethanol / 15.5 h / 20 °C

3.2: 1 h / 20 °C

With piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; potassium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1002/chem.201101015