N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

Base Information

Chemical Name:N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide
CAS No.:698351-25-6
Molecular Formula:C₁₃H₁₅FN₂OS
Molecular Weight:266.339
Hs Code.:

Synonyms:N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

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Chemical Property of N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

Chemical Property:

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Technology Process of N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

There total 3 articles about N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26391-06-0
2-cyano-N,N-diethylacetamide

: 698351-25-6
N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 2 h / -78 °C

1.2: tetrahydrofuran / 9 h / 20 °C

2.1: 9.2 g / 1-fluoropyridinium trifluoromethanesulfonate / CH₂Cl₂ / 13 h

3.1: LDA / tetrahydrofuran / 1 h / -78 °C

3.2: 1.37 mg / tetrahydrofuran / 9 h / 20 °C

With N-fluoropyridinium triflate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 698351-77-8
2-cyano-N,N-diethyl-2-fluoro-acetamide

: 698351-25-6
N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

Guidance literature:: 2-cyano-N,N-diethyl-2-fluoro-acetamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

benzenesulfenyl chloride; In tetrahydrofuran; at 20 ℃; for 9h;

Reference yield:

: (Z)-3-Diethylamino-3-trimethylsilanyloxy-acrylonitrile

: 698351-25-6
N,N-diethyl 2-cyano-2-fluoro-2-phenylthioacetoamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9.2 g / 1-fluoropyridinium trifluoromethanesulfonate / CH₂Cl₂ / 13 h

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: 1.37 mg / tetrahydrofuran / 9 h / 20 °C

With N-fluoropyridinium triflate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;