2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine
CAS No.:1403783-44-7
Molecular Formula:C₃₃H₄₀ClNO₂
Molecular Weight:518.139
Hs Code.:

Synonyms:2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

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Chemical Property of 2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

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Technology Process of 2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

There total 8 articles about 2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1403783-45-8
C₁₈H₂₁N₃O₂

: 1403783-46-9
1-chloro-4-(3-cyclohexylprop-1-en-2-yl)benzene

: 1403783-44-7
2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: In neat (no solvent); at 72 ℃; for 3.5h;
DOI:10.1016/j.tet.2012.08.089

Reference yield:

: 87482-75-5
1-(4-chlorophenyl)-2-cyclohexylethan-1-one

: 1403783-44-7
2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / diethyl ether / 0.5 h / 20 °C

1.2: 4 h / 20 °C

2.1: neat (no solvent) / 3.5 h / 72 °C

With potassium tert-butylate; In diethyl ether; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination;
DOI:10.1016/j.tet.2012.08.089

Reference yield:

: 1226012-35-6
(4-(2-(dimethylamino)ethoxy)phenyl)(4-methoxyphenyl)methanone

: 1403783-44-7
2-(4-(2-(4-chlorophenyl)-2-(cyclohexylmethyl)-1-(4-methoxyphenyl)-cyclopropyl)phenoxy)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 24 h / Reflux

2: sodium sulfate; potassium hydroxide; mercury(II) oxide / ethanol; diethyl ether / 1 h / 20 °C / Darkness

3: neat (no solvent) / 3.5 h / 72 °C

With hydrazine hydrate; sodium sulfate; potassium hydroxide; mercury(II) oxide; In diethyl ether; ethanol;
DOI:10.1016/j.tet.2012.08.089