2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

Base Information

Chemical Name:2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester
CAS No.:1173893-39-4
Molecular Formula:C₁₆H₂₀ClNO₂
Molecular Weight:293.793
Hs Code.:

Synonyms:2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

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Chemical Property of 2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

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Technology Process of 2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

There total 1 articles about 2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 106-95-6
allyl bromide

: 166655-36-3
{[1-(4-chlorophenyl)methylidene]amino}acetic acid tert-butyl ester

: 1173893-39-4
2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

Guidance literature:: {[1-(4-chlorophenyl)methylidene]amino}acetic acid tert-butyl ester; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.666667h;

allyl bromide; In tetrahydrofuran; hexane; at -78 ℃;
DOI:10.1016/j.tetlet.2009.04.099

Reference yield: 74.0%

: 12082-05-2
(η6-fluorobenzene)tricarbonylchromium

: 1173893-39-4
2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

: 848829-60-7
(S)-2-allyl-2-phenylglycine t-butyl ester

Guidance literature:: (η6-fluorobenzene)tricarbonylchromium; 2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester; With (11bR)-(+)-4,4-dibutyl-4,5-dihydro-2,6-bis(3,4,5-trifluorophenyl)-3H-dinaphth[2,1-c:1′,2′-e]azepinium bromide; cesium hydroxide; In water; toluene; at 0 ℃; for 24h;

With hydrogenchloride; In water; at 20 ℃; for 12h; enantioselective reaction;
DOI:10.1002/anie.201409065

Reference yield: 62.3%

: 1173893-39-4
2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester

: 184773-89-5
1-bromo-4-(3-bromoprop-1-en-2-yl)benzene

: 1173893-40-7
(R)-2-allyl-2-amino-4-(4-bromophenyl)pent-4-enoic acid tert-butyl ester

Guidance literature:: 2-{[1-(4-chlorophenyl)methylidene]amino}pent-4-enoic acid tert-butyl ester; 1-bromo-4-(3-bromoprop-1-en-2-yl)benzene; With (11bS,11b’S)-2,6-bis(3,4,5-trifluorophenyl)-3,3’,5,5’-tetrahydro-4,4’-spirobi[dinaphtho[2,1-c:1’,2’-e]azepin]-4-ium bromide; caesium hydroxide monohydrate; In toluene; at -10 - -5 ℃; for 24h;

With citric acid; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2009.04.099