3,3''-DIAZIDOBENZOPHENONE

Base Information

• Chemical Name: 3,3''-DIAZIDOBENZOPHENONE
• CAS No.: 112028-53-2
• Molecular Formula: C13H8 N6 O
• Molecular Weight: 264.24222
• Mol file: 112028-53-2.mol

Synonyms:3,3'-Diazidobenzophenone

Chemical Property of 3,3''-DIAZIDOBENZOPHENONE

Chemical Property:

• PSA: 116.57000
• LogP: 3.70672

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3''-DIAZIDOBENZOPHENONE

There total 1 articles about 3,3''-DIAZIDOBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-dinitrobenzophenone (21222-05-9) → 3,3'-diazidobenzophenone (112028-53-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / SnCl₂*2H₂O / ethanol / 0.5 h / 70 °C

2: 1.) aq. HCl, NaNO₂, 2.) NaN₃ / 1.) 0 deg C, 1 h

With hydrogenchloride; sodium azide; tin(ll) chloride; sodium nitrite; In ethanol;

Reference yield:

3,3'-diazidobenzophenone (112028-53-2) → 3,3'-dinitrenobenzophenone tetraradical

Guidance literature:

In 2-methyltetrahydrofuran; at -196.1 ℃; Irradiation;

upstream raw materials:

3,3'-dinitrobenzophenone

Refernces