[(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

Base Information

Chemical Name:[(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester
CAS No.:172034-33-2
Molecular Formula:C₁₆H₁₉Cl₂NO₄
Molecular Weight:360.237
Hs Code.:

Synonyms:[(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

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MSDS Files:: SDS file from LookChem

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Technology Process of [(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

There total 1 articles about [(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 79-36-7
dichloroacethyl chloride

: 72155-45-4
Boc-L-phenylalaninal

: 172034-33-2
[(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 25 ℃; for 6h;
DOI:10.1039/c39950001735

Reference yield: 97.0%

: 172034-33-2
[(S)-1-((R)-3,3-Dichloro-4-oxo-oxetan-2-yl)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

: 172034-34-3
(4S)-4-<(1S)-<(tert-butoxycarbonyl)amino>-2-phenylethyl>oxetan-2-one

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; for 24h; under 760 Torr;
DOI:10.1021/jo961219s