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Technology Process of ((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

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  • Chemical Name:((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)
  • CAS No.:623924-17-4
  • Molecular Formula:C42H58F3N3O3STi
  • Molecular Weight:789.882
  • Hs Code.:
((2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>)NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)N(2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>))Ti=NC<sub>6</sub>H<sub>3</sub>-2,6-[CH(CH<sub>3</sub>)2]2(OTf)

Synonyms:((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

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Chemical Property of ((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)
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Technology Process of ((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

There total 4 articles about ((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

Ti(CH(C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)(HNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2
623924-14-1

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2

silver trifluoromethanesulfonate
2923-28-6

silver trifluoromethanesulfonate

((2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>)NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)N(2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>))Ti=NC<sub>6</sub>H<sub>3</sub>-2,6-[CH(CH<sub>3</sub>)2]2(OTf)
623924-17-4

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

Guidance literature:
In tetrahydrofuran; at 25°C for 1 h or longer;
DOI:10.1039/b304633h

Reference yield:

[([2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>]NC(Me)CHC(Me)N[2,6-iPr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>])TiCl<sub>2</sub>·THF]
543740-53-0

[([2,6-iPr2C6H3]NC(Me)CHC(Me)N[2,6-iPr2C6H3])TiCl2·THF]

((2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>)NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)N(2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>))Ti=NC<sub>6</sub>H<sub>3</sub>-2,6-[CH(CH<sub>3</sub>)2]2(OTf)
623924-17-4

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

Guidance literature:
Multi-step reaction with 2 steps
1: diethyl ether
2: tetrahydrofuran
In tetrahydrofuran; diethyl ether;
DOI:10.1039/b304633h

Reference yield:

Ti(CH(C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)(HNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2
623924-14-1

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2

((2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>)NC(CH<sub>3</sub>)CHC(CH<sub>3</sub>)N(2,6-[CH(CH<sub>3</sub>)2]2C<sub>6</sub>H<sub>3</sub>))Ti=NC<sub>6</sub>H<sub>3</sub>-2,6-[CH(CH<sub>3</sub>)2]2(OTf)
623924-17-4

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

Guidance literature:
Multi-step reaction with 2 steps
1: tetrahydrofuran
2: dichloromethane
In tetrahydrofuran; dichloromethane;
DOI:10.1039/b304633h
upstream raw materials:

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2

silver trifluoromethanesulfonate

Ti(CH(C(CH3)NC6H3(CH(CH3)2)2)2)(HNC6H3(CH(CH3)2)2)2(1+)*B(C6F5)4(1-)=Ti(CH(C(CH3)NC6H3(C3H7)2)2)(HNC6H3(C3H7)2)2B(C6F5)4

thallium(I) triflate

Downstream raw materials:

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(O)=CPh2C(CH3)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OTf)

((2,6-[CH(CH3)2]2C6H3)NC(CH3)CHC(CH2)N(2,6-[CH(CH3)2]2C6H3))Ti=NC6H3-2,6-[CH(CH3)2]2(OEt2)

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