ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

Base Information

Chemical Name:ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate
CAS No.:211812-06-5
Molecular Formula:C₂₀H₂₇NO₆
Molecular Weight:377.437
Hs Code.:

Synonyms:ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

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Chemical Property of ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

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Technology Process of ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

There total 5 articles about ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98-88-4
benzoyl chloride

: 211812-05-4
ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)aminooxy]-2-penteneoate

: 211812-06-5
ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jo980654e

Reference yield:

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 211812-06-5
ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / KOH / ethanol / 60 °C

2: 67 percent / diethyl ether

3: PDC, molecular sieves / CH₂Cl₂ / 18 h / Ambient temperature

4: hexane / 12 h / Heating

5: 97 percent / Et₃N / CH₂Cl₂

With potassium hydroxide; dipyridinium dichromate; molecular sieve; triethylamine; In diethyl ether; ethanol; hexane; dichloromethane;
DOI:10.1021/jo980654e

Reference yield:

: 211812-04-3
N-Boc-2-aminooxy-2-methylpropan-1-ol

: 211812-06-5
ethyl 4-methyl-4-[N-(tert-butoxycarbonyl)-N-(benzoyl)aminooxy]-2-penteneoate

Guidance literature:: Multi-step reaction with 3 steps

1: PDC, molecular sieves / CH₂Cl₂ / 18 h / Ambient temperature

2: hexane / 12 h / Heating

3: 97 percent / Et₃N / CH₂Cl₂

With dipyridinium dichromate; molecular sieve; triethylamine; In hexane; dichloromethane;
DOI:10.1021/jo980654e