Technology Process of C17H15Br2NO2
There total 6 articles about C17H15Br2NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bromine;
hydrogen bromide;
In
dichloromethane; acetic acid;
at 35 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 °C
2: diethyl ether; tetrahydrofuran / -70 - 20 °C
3: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / ISOPROPYLAMIDE / 20 h / 85 °C / Inert atmosphere
4: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; ethanol; water / 5 h / 115 °C / Inert atmosphere
5: bromine / hydrogen bromide / dichloromethane; acetic acid / 35 °C
With
bromine; potassium acetate; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
tetrakis(triphenylphosphine) palladium(0); hydrogen bromide;
In
tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; ethanol; dichloromethane; ISOPROPYLAMIDE; water; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate / tetrakis(triphenylphosphine) palladium(0) / ISOPROPYLAMIDE / 20 h / 85 °C / Inert atmosphere
2: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; ethanol; water / 5 h / 115 °C / Inert atmosphere
3: bromine / hydrogen bromide / dichloromethane; acetic acid / 35 °C
With
bromine; potassium acetate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); hydrogen bromide;
In
1,2-dimethoxyethane; ethanol; dichloromethane; ISOPROPYLAMIDE; water; acetic acid;