5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

Base Information

Chemical Name:5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide
CAS No.:362011-06-1
Molecular Formula:C₆₆H₇₇I
Molecular Weight:997.242
Hs Code.:

Synonyms:5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

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Chemical Property of 5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

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Technology Process of 5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

There total 2 articles about 5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21521-51-7
2,4,6-tribromoiodobenzene

: 362011-06-1
5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran

1.2: tetrahydrofuran

1.3: 67 percent / H⁽¹⁺⁾ / tetrahydrofuran

2.1: Mg / tetrahydrofuran

2.2: tetrahydrofuran

2.3: 69 percent / I₂ / tetrahydrofuran

With magnesium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)00871-1

Reference yield:

: 57190-17-7
2-bromo-1,3-diisopropylbenzene

: 362011-06-1
5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran

1.2: tetrahydrofuran

1.3: 67 percent / H⁽¹⁺⁾ / tetrahydrofuran

2.1: Mg / tetrahydrofuran

2.2: tetrahydrofuran

2.3: 69 percent / I₂ / tetrahydrofuran

With magnesium; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)00871-1

Reference yield: 86.2%

: 362011-06-1
5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide

: 796055-70-4
5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl-SeH

Guidance literature:: 5',5'''-bis(2,6-diisopropylphenyl)-2,6,2'''',6''''-tetraisopropyl-m-quinquephenyl-2''-yl iodide; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -76 ℃; for 0.5h;

With selenium; In tetrahydrofuran; pentane; at -76 - 20 ℃;

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja0457009