(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

Base Information

Chemical Name:(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid
CAS No.:1446115-09-8
Molecular Formula:C₂₁H₂₈N₂O₅S
Molecular Weight:420.53
Hs Code.:

Synonyms:(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

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Chemical Property of (S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

Chemical Property:

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Technology Process of (S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

There total 4 articles about (S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56-45-1,83245-15-2
L-serin

: 1429346-18-8
N-(2,4-dimethylphenyl)-4-fluoro-N-isobutylbenzenesulfonamide

: 1446115-09-8
(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; mineral oil; for 2h; Inert atmosphere;

Reference yield:

: 95-68-1
2,4-Xylidine

: 1446115-09-8
(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium iodide; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] / water / 1 h / 170 °C / Microwave irradiation

2: pyridine / 16 h / 20 °C

3: sodium hydride / mineral oil; dimethyl sulfoxide / 122 h / 20 °C / Inert atmosphere

With pyridine; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium hydride; potassium iodide; In water; dimethyl sulfoxide; mineral oil;

Reference yield:

: (2,4-dimethylphenyl)(2-methylpropyl)amine

: 1446115-09-8
(S)-2-((4-(N-(2,4-dimethylphenyl)-N-isobutylsulfamoyl)phenyl)amino)-3-hydroxypropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h / 20 °C

2: sodium hydride / mineral oil; dimethyl sulfoxide / 122 h / 20 °C / Inert atmosphere

With pyridine; sodium hydride; In dimethyl sulfoxide; mineral oil;