1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine

Base Information

• Chemical Name: 1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine
• CAS No.: 1213230-43-3
• Molecular Formula: C₂₀H₃₉N₅
• Molecular Weight: 349.563

Synonyms:1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine

Chemical Property of 1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine

Chemical Property:

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Technology Process of 1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine

There total 2 articles about 1,6-dihydro-6,6-dimethyl-N₄-octyl-N₂-cyclohexyl-N₂-methyl-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N5-octyl-N1-cyclohexyl-N1-methyl-biguanide hydrochloride (1213230-68-2) + acetone (67-64-1) → 1,6-dihydro-6,6-dimethyl-N4-octyl-N2-cyclohexyl-N2-methyl-1,3,5-triazine-2,4-diamine (1213230-43-3)

Guidance literature:

N₅-octyl-N₁-cyclohexyl-N₁-methyl-biguanide hydrochloride; acetone; With sulfuric acid; In ethanol; for 20h; Reflux;

With sodium hydroxide; In ethanol; water; for 2h; Reflux;

Reference yield:

N-octyl-N'-cyanoguanidine (60852-95-1) + N-methyl-cyclohexanamine hydrochloride (65845-61-6) → 1,6-dihydro-6,6-dimethyl-N4-octyl-N2-cyclohexyl-N2-methyl-1,3,5-triazine-2,4-diamine (1213230-43-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride / water; xylene / 6 h / Reflux

2.1: sulfuric acid / ethanol / 20 h / Reflux

2.2: 2 h / Reflux

With hydrogenchloride; sulfuric acid; In ethanol; water; xylene;

upstream raw materials:

N-octyl-N'-cyanoguanidine

N-methyl-cyclohexanamine hydrochloride

N₅-octyl-N₁-cyclohexyl-N₁-methyl-biguanide hydrochloride

acetone

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