1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

Base Information

Chemical Name:1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane
CAS No.:227000-80-8
Molecular Formula:C₂₅H₃₉NO₂Si
Molecular Weight:413.676
Hs Code.:

Synonyms:1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

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Technology Process of 1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

There total 6 articles about 1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 227000-46-6
1-trimethylsilyloxy-2,2,5-trimethyl-4-phenyl-3-azahexane 3-nitroxide

: 227000-80-8
1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

Guidance literature:: (1-bromoethyl)benzne; With hydrazine; sonicated;

1-trimethylsilyloxy-2,2,5-trimethyl-4-phenyl-3-azahexane 3-nitroxide; With lead dioxide; In toluene; at 0 - 20 ℃;
DOI:10.1081/SCC-120039497

Reference yield:

: 227000-16-0
N-(2-hydroxy-1,1-dimethylethyl)-α-isopropylnitrone

: 227000-80-8
1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / pyridine / diethyl ether / 12 h / Ambient temperature

2: 2.) conc. aq. NH₃, Cu(OAc₂)2, air / 1.) THF, Et₂O, RT, 2 h, 2.) THF, Et₂O, methanol, 30 min

3: 1.) PbO₂ / 1.) toluene, 5 min, irrad., 2.) toluene, from -78 deg C to RT, 1 h

With pyridine; ammonium hydroxide; air; Cu(OAc₂)2; lead dioxide; In diethyl ether;
DOI:10.1021/ja984013c

Reference yield:

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 227000-80-8
1-trimethylsilyloxy-2,2,5-trimethyl-3-(1-phenylethoxy)-4-phenyl-3-azahexane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine

2: 1.) PbO₂ / 1.) toluene, 5 min, irrad., 2.) toluene, from -78 deg C to RT, 1 h

With lead dioxide; hydrazine;
DOI:10.1021/ja984013c