Technology Process of C19H23N5O6S
There total 7 articles about C19H23N5O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonia / tetrahydrofuran; water / 1.3 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
With
ammonia; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: trichlorophosphate; N,N-dimethyl-aniline / 2 h / 0 - 100 °C
2: triethylamine; ammonia / tetrahydrofuran; isopropyl alcohol / 5 h / 20 °C
3: triethylamine / tetrahydrofuran / 6 h / 20 °C
4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C
5: ammonia / tetrahydrofuran; water / 1.3 h / 20 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
With
di-isopropyl azodicarboxylate; ammonia; N,N-dimethyl-aniline; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; water; isopropyl alcohol;