2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

Base Information

Chemical Name:2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside
CAS No.:959922-41-9
Molecular Formula:C₂₃H₃₂O₇
Molecular Weight:420.503
Hs Code.:

Synonyms:2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

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Technology Process of 2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

There total 2 articles about 2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 959922-39-5
4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-galactopyranoside

: 2622-05-1
allylmagnesium bromide

: 959922-41-9
2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

Guidance literature:: 4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-galactopyranoside; With pyridine-SO₃ complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;

allylmagnesium bromide; In tetrahydrofuran; at -78 ℃; Further stages.;
DOI:10.1002/anie.200703027

Reference yield:

: C₂₀H₂₆O₇

: 2622-05-1
allylmagnesium bromide

: 959922-41-9
2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

Guidance literature:: In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1002/chem.200801103

Reference yield: 92.0%

: 959922-41-9
2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

: 100-39-0
benzyl bromide

: 959922-22-6
2-allyl-2-O-benzyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside

Guidance literature:: 2-allyl-4,6-O-benzylidene-3-O-methoxymethyl-(pent-4-enyl)-β-D-talopyranoside; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.75h;

benzyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/chem.200801103