5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II)

Base Information

• Chemical Name: 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II)
• CAS No.: 1073711-41-7
• Molecular Formula: C₆₇H₇₅N₅Ni
• Molecular Weight: 1009.06

Synonyms:5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II)

Chemical Property of 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II)

Chemical Property:

Purity/Quality:

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Technology Process of 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II)

There total 1 articles about 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodopyridine (5029-67-4) + 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(3,3,4,4-tetramethyl-2,5-dioxaboranyl)porphyrinatonickel(II) (1073711-40-6) → 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II) (1073711-41-7)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; triphenylphosphine; In water; N,N-dimethyl-formamide; toluene; Pd2(dba)3, PPh3, Cs2CO3, CsF, toluene/DMF/H2O, reflux;

DOI:10.1021/ja8066385

Reference yield: 64.0%

potassium tetrachloroplatinate(II) (10025-99-7) + 5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II) (1073711-41-7) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → [Ni(C20H7N4(C6H3(C(CH3)3)2)3(C5H4N)Pt(OC(H)N(CH3)CH2))] (1111326-28-3)

Guidance literature:

With NaO₂CCH₃; In N,N-dimethyl-formamide; toluene; mixt. of Ni complex, Pt complex and NaOAc in toluene/DMF heated at 100°C;

DOI:10.1021/ic8019149

Reference yield: 23.0%

5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II) (1073711-41-7) + lithium phenylacetylide (4440-01-1) → C75H79N5Ni (1377786-72-5)

Guidance literature:

5,10,15-tris(3,5-di-tert-butylphenyl)-18-(2-pyridyl)porphyrinatonickel(II); lithium phenylacetylide; In tetrahydrofuran; at 20 ℃; for 12h;

With water;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone;

DOI:10.1021/ol301005b

upstream raw materials:

2-iodopyridine

5,10,15-tris(3,5-di-tert-butylphenyl)-18-(3,3,4,4-tetramethyl-2,5-dioxaboranyl)porphyrinatonickel(II)

Downstream raw materials:

[Ni(C₂₀H₇N₄(C₆H₃(C(CH₃)3)2)3(C₅H₄N)PtCl(CO))]

[Ni(C₂₀H₇N₄(C₆H₃(C(CH₃)3)2)3(C₅H₄N)Pt(OC(H)N(CH₃)CH₂))]

C₇₅H₇₉N₅Ni

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